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The supernatants were lyophilized and derivatized with methoxyamine hydrochloride, pyridine, and N-methyl-N-(trimethylsilyl)trifluoroacetamide, before being analyzed by gas chromatography time-of-flight mass spectrometry (GC-TOF-MS)

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[DOI] [PMC free article] [PubMed] [Google Scholar] 149.Genazzani A.D., Prati A., Marchini F., Petrillo T., Napolitano A., Simoncini T