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Description
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Amino acids and biogenic amines were quantified using liquid chromatography coupled with tandem mass spectrometry (LC-MS/MS), while acylcarnitines, lipids and hexoses were analyzed by flow injection analysis mass spectrometry (FIA-MS/MS) on an ABI 4000 Q-Trap mass spectrometer (Applied Biosystems)
In the method 1, a solution of Aminooxy corresponding to the desired quantities (0.1 to 1 equivalent relative to Au 15 SG 13 ) was added to a water solution of Au 15 SG 13 (1 mg/ml, pH ~ 8.5)
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