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The resulting extracts were analysed by ultrahigh performance liquid chromatographytandem mass spectroscopy (UPLC-MS/MS) using a Waters ACQUITY ultra-performance liquid chromatography (UPLC) and a Thermo Scientific Q-Exactive high resolution/accurate mass spectrometer (MS) interfaced with a heated electrospray ionisation (HESI-II) source and Orbitrap mass analyzer operated at 35,000 mass resolution 60

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