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By comparing the Hg-TPD patterns of pristine PPS, unsaturated Se/PPS-I (adsorption of Hg 0 for 2 h), and selenium powder +PPS, it was found that the characteristic peak at ~ 160 C was attributed to the chemical interaction between PPS-sulfur and mercury (no physisorption was accounted considering the high pretreatment and decomposition temperature), and the one centered at ~ 230 C was ascribed to HgSe 12

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