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The analytes were eluted by the mobile phase containing (A) 0.1% TCA adjusted to pH 1.7 with 1 mol/L NaOH and (B) ACN with the gradient elution as follows: 06 min, 1935% (B)

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Acknowledgements This manuscript was completed with project funding from Changxiang Li, Qingguo Wang and Zilin Ren

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