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The mobile phase conditions employed were as follows: MS grade 0.1 per cent formic acid (aqueous) for Solvent A, MS grade acetonitrile for Solvent B, 0.5mLmin 1 flow rate, 40C column temperature
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Four hours later, the symptoms suddenly flared up to 10, but I found that I preferred this dramatic seesawing to the gradual return of symptoms I experienced after using other remedies
