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From L-malic acid ( S )-Acetoxypyrrolidin-2,5-dione ( 51 ), readily available from L-malic acid [62], was carefully reduced and immediately acetylated to ( S )- 52 which was reacted with furan to produce a 67:33 mixture of readily separable (2 S ,3 S )- 53 and (2 R ,3 S )- 53 , respectively

The reduction phase involves two subsequent steps, the first producing a glutathionylated intermediate GPX enzyme where the oxidized GPX reacts with the first equivalent of GSH